HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 66599945, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 59548884 | HCID 59548884 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66599945 | HCID 66599945 | 100% |
Reaction Steps
To a vial containing 4-(2-phenylcarbamoyl-phenyl)-piperazine-1-carboxylic acid tert-butyl ester (0.438 g, 1.150 mmol) is added 2 mL of CH2Cl2 and 2 mL of TFA. The mixture stirred for 1 h and then concentrated to dryness to give 0.454 g of 4-(2-phenylcarbamoyl-phenyl)-piperazine trifluroacetate in 100% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08362249B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-fcf02e9dad5847d3b7d528cfc7d19a26 |
| Source note | uspto-grants-2013_01 |