2-Methoxyethylamine → HCID 25177309, compound

Participants

Reaction Steps

According to the method of Example 2-14 except that 2-methoxyethylamine (15 μl, 0.175 mmol) was used instead of methylamine, (S)-4-amino-18,20-dimethyl-10,16-dioxo-7-thia-3,5,11,15-tetraazatricyclo[15.3.1.12,6]docosa-1(20),2(22),3,5,17(21),18-hexaene-14-carboxylic acid (2-methoxyethyl)amide (Compound 66) (16 mg) was obtained as a white solid material from (S)-4-amino-18,20-dimethyl-10,16-dioxo-7-thia-3,5,11,15-tetraazatricyclo[15.3.1.12,6]docosa-1(20),2(22),3,5,17(21),18-hexaene-14-carboxylic acid (25 mg, 0.058 mmol) obtained in Example 2-13.

Provenance & Evidence