HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20770804, compound → HCID 20770800, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20770804 | HCID 20770804 | — |
| Reactant | HCID 20770807 | HCID 20770807 | — |
| Reactant | HCID 22280116 | HCID 22280116 | — |
| Product | HCID 20770800 | HCID 20770800 | 25% |
Reaction Steps
Compound 76D was prepared analogously to compound 21D using the product prepared from compound 76C and 6B. Yield was 25% after flash column purification. MS m/z 504 (M+1). 400 MHz 1H NMR (DMSO-d6) δ 7.61-6.71 (m, 11H), 5.05 (s, 2H), 4.50 (s, 2H), 3.99 (s, 2H), 3.74 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06875780B2 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-6d5674adbd55413d89697c875c7a41f8 |
| Source note | uspto-grants-2005_04 |