HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 1-Bromo-2-methoxy-3-nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Bromo-6-nitrophenol | HCID 13545453 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 1-Bromo-2-methoxy-3-nitrobenzene | HCID 22505713 | — |
Reaction Steps
A mixture of 2-bromo-6-nitrophenol (10.8 g; 0.0495 mol.), methyl iodide (3.4 mL; 0.00545 mol.) and potassium carbonate (8.2 g; 0.0592 mol.) in acetone (250 mL) was stirred and heated under reflux for 24 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06875786B2 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-1e03a1ea4eea434e9b2261565b8eb06e |
| Source note | uspto-grants-2005_04 |