p-Toluenesulfonic acid → HCID 178516922, compound

Participants

Reaction Steps

To a solution of the product from step b) (0.30 g) in dry toluene (60 ml) was added p-toluene sulphonic acid (50 mg) and the solution heated under reflux for 11 hours. The resultant solid was collected by filtration, washed with ether and dried to give the subtitle compound as a colourless solid (0.290 g)

Provenance & Evidence