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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1814277Generated: November 2, 2026

HCID 87952601, compound → HCID 22504144, compound

https://huagongshe.com/reaction/1814277

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 87952601HCID 87952601—
SolventDichloromethaneHCID 6344—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 22504144HCID 22504144—

Reaction Steps

A solution of 3-[4-acetylamino-2-(2-naphthalen-1-yl-ethoxy)-benzenesulfonylamino]-4-oxo-butyric acid tert-butyl ester (110 mg) in methylene chloride (6 mL) and trifluoroacetic acid (3 mL) was stirred at room temperature for 4 hours. The solvent was evaporated. The residue was triturated with ether and the resulting amorphous solid (58 mg) was collected by filtration.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06875765B2
Source datasetuspto-grants-2005_04
ORD IDord-8bb7821d60034dd5a2522685ae573648
Source noteuspto-grants-2005_04