HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 87952601, compound → HCID 22504144, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 87952601 | HCID 87952601 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 22504144 | HCID 22504144 | — |
Reaction Steps
A solution of 3-[4-acetylamino-2-(2-naphthalen-1-yl-ethoxy)-benzenesulfonylamino]-4-oxo-butyric acid tert-butyl ester (110 mg) in methylene chloride (6 mL) and trifluoroacetic acid (3 mL) was stirred at room temperature for 4 hours. The solvent was evaporated. The residue was triturated with ether and the resulting amorphous solid (58 mg) was collected by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06875765B2 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-8bb7821d60034dd5a2522685ae573648 |
| Source note | uspto-grants-2005_04 |