HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1814627Erstellt: 25. Oktober 2026
Potassium Phosphate, Dibasic → HCID 22501863, Verbindung
https://huagongshe.com/reaction/1814627
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Potassium Phosphate, Dibasic | HCID 24450 | — |
| Edukt | Monobasic potassium phosphate | HCID 516951 | — |
| Edukt | Ethyl 3-[5-bromomethyl-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl]propionate | HCID 22502293 | — |
| Lösungsmittel | Dimethyl Sulfoxide | HCID 679 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | HCID 22501863 | HCID 22501863 | — |
Reaktionsschritte
The crude material from step 2 was dissolved in DMSO (70 mL). Powdered K2HPO4 (18 g, 0.10 mol) and KH2PO4 (7 g, 0.05 mol) were added. The mixture was stirred at 80° C. for 5 hours, diluted with water (500 mL), and extracted with ethyl acetate (3×100 mL). The combined organic extracts were dried (MgSO4), and concentrated. After column chromatography (hexane, ethyl acetate 3:1) 4.8 g of the title compound was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US06875760B2 |
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| Quelldatensatz | uspto-grants-2005_04 |
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| ORD ID | ord-ec78bd0d12954bc2ba2ae6fc04debc21 |
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| Quellennotiz | uspto-grants-2005_04 |
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