HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloride → HCID 11401639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloride | HCID 312 | — |
| Reactant | DL-alanine | HCID 602 | — |
| Reactant | Octanoyl chloride | HCID 8124 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Product | HCID 11401639 | HCID 11401639 | — |
Reaction Steps
The preparation is carried out analogously to the procedure of example 1A using 16.5 g (0.185 mol) of D,L-alanine, 41.23 g (0.407 mol) of triethylamine, 44.27 g (0.407 mol) of trimethylsilyl)l chloride and 30.12 g (0.185 mol) of octanoyl chloride. The product crystallizes from toluene/n-hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06878708B2 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-0a1f75fda78c4b0da530f08bb9fe7766 |
| Source note | uspto-grants-2005_04 |