HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 135604937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 2,5-Dichlorothiophene-3-sulfonyl chloride | HCID 2736094 | — |
| Reactant | 2-(5-Amino-2-propoxyphenyl)-5-methyl-7-cyclopentyl-3H-imidazo[5,1-f][1,2,4]-triazin-4-one | HCID 135604925 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 135604937 | HCID 135604937 | — |
Reaction Steps
150 mg (0.408 mmol) of the compound from example 44A are reacted with 308 mg (1.224 mmol) of 2,5-dichlorothiophene-3-sulfonyl chloride and 0.33 ml (4.08 mmol) of pyridine in tetrahydrofuran for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06878708B2 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-d4fdb73c34e24e6ea726d5ad6b79e1bf |
| Source note | uspto-grants-2005_04 |