HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Isocyanato-4-[(trifluoromethyl)sulfanyl]benzene → HCID 135604947, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Isocyanato-4-[(trifluoromethyl)sulfanyl]benzene | HCID 2733392 | — |
| Reactant | HCID 135843655 | HCID 135843655 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 135604947 | HCID 135604947 | — |
Reaction Steps
Analogously to the procedure of example 54, 230 mg (0.647 mmol) of the amino compound from example 48A are reacted with 284 mg (1.29 mmol) of 4-(trifluoromethylthio)phenyl isocyanate in 20 ml of tetrahydrofuran for 4 hours. The crude product is purified by silica gel chromatography using toluene and ethyl acetate as mobile phase.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06878708B2 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-a64469d75bc944e4b9d34ee46fa5ace9 |
| Source note | uspto-grants-2005_04 |