HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53951389, compound → HCID 53803790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53951389 | HCID 53951389 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53803790 | HCID 53803790 | — |
Reaction Steps
A solution of the (R)-1-(5-azidohexyl)-3,7-dimethylxanthine (620 mg) in ethanol (25 ml) was hydrogenated at 70 psi of hydrogen gas in presence of 10% palladium on carbon (150 mg) for 12 hours. After filtration to remove the catalyst, the filtrate was concentrated under reduced pressure to provide (R)-1-(5-aminohexyl)-3,7-dimethylxanthine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06878715B1 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-05f1241752ae45dfac9c0a24fd76ffc9 |
| Source note | uspto-grants-2005_04 |