Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 54165680 | HCID 54165680 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54538731 | HCID 54538731 | — |
Reaction Steps
(R)-1-(5-Hydroxyhexyl)-7-ethoxymethyl-8-amino-3-methylxanthine libraries synthesized as described in Example 33 were treated with a solution composed of concentrated hydrochloric acid and ethanol (1:4, 0.8 ml per well) and the block was heated in an oven at 80° C. for 12 hours. Remaining reagents and byproducts were evaporated under reduced pressure providing (R)-1-(5-hydroxyhexyl)-8-amino-3-methylxanthine libraries.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06878715B1 |
|---|
| Source dataset | uspto-grants-2005_04 |
|---|
| ORD ID | ord-1bd7f263aaa84a1db11be54d63a27c8c |
|---|
| Source note | uspto-grants-2005_04 |
|---|