HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 22144861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | HCID 69627321 | HCID 69627321 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22144861 | HCID 22144861 | — |
Reaction Steps
Beginning with pent-2-en-1-yl 2-bromo-4-fluorophenyl ether, the title compound was prepared essentially as described in Preparation XVII, except that Amberlyst 15™ resin in refluxing toluene was used in place of sulfuric acid, and water was removed by azeotropic distillation with a Dean-Stark trap.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06881733B1 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-31e329c4268c48d18a3a38db122f0212 |
| Source note | uspto-grants-2005_04 |