HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzyl-3-methyl-4-piperidone → HCID 22495572, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzyl-3-methyl-4-piperidone | HCID 560965 | — |
| Reactant | 7-Bromo-6-fluoro-1-benzofuran | HCID 22144929 | — |
| Product | HCID 22495572 | HCID 22495572 | 59.3% |
Reaction Steps
Beginning with 5.22 gm (24.3 mMol) 6-fluoro-7-bromobenzofuran and 5.19 gm (25.5 mMol) 1-benzyl-3-methyl-4-oxopiperidine, 4.89 gm (59%) of the desired compound were prepared as a mixture of cis- and trans-isomers, essentially as described in EXAMPLE 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06881733B1 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-6249c11d38cb4dfdb0a156aecefb30b5 |
| Source note | uspto-grants-2005_04 |