HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 12985380, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 86759657 | HCID 86759657 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 12985380 | HCID 12985380 | 96% |
Reaction Steps
The product from step B (0.26 g, 0.30 mmol) and Pd/C (10%, 0.026 g) were mixed with methanol (5 mL) and placed under a hydrogen atmosphere for 18 h. The mixture was filtered and evaporated to give a yellowish solid (0.155 g, 96%): mp 84-88° C.; LC/MS (+APCI) m/z 263 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06881749B2 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-4f19b10671164383a40aa7aaf38257aa |
| Source note | uspto-grants-2005_04 |