2-Adamantanol → 2-Adamantanol

Participants

Reaction Steps

After the completion of the reaction, the produced liquid was analyzed by means of gas chromatogram (available from Shimadzu GC-14A column, PEG=20 M, capillary column). As a result, there were obtained as the objective products, 93.8 μmol of 1-adamantanol, 22.2 μmol of 2-adamantanone and 75.7 μmol of 2-adamantanol at a yield of 19.2% with selectivity to 2-adamantanone and 2-adamantanol of 51.1%. The performance results are given in Table 1.

Provenance & Evidence