HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 3544473, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 3557290 | HCID 3557290 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 3544473 | HCID 3544473 | — |
Reaction Steps
3-Dimethylamino-2-(2-nitrophenyl)propenal (Maybridge) in ethanol was treated with hydrazine via syringe and heated to reflux for 16 hours. Concentration in vacuo afforded crude 4-(2-nitrophenyl)pyrazole, which was reduced as in Example 64 and coupled with CMI to give the fumaric acid salt of N-(4,5-dihydro-1H-imidazol-2-ylmethyl)-2-(1H-pyrazol-4-yl)aniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06884801B1 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-a633342630a0411fb0898a68c189538d |
| Source note | uspto-grants-2005_04 |