HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22494651, compound → UUKHAODJZMXSOX-UHFFFAOYSA-N
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22494651 | HCID 22494651 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | UUKHAODJZMXSOX-UHFFFAOYSA-N | HCID 22494678 | 109.6% |
Reaction Steps
A solution of 4-(2-cyclohexenyloxy)-N-(benzyloxycarbonyl)piperidine (3.80 g), and 10% palladium on carbon (50% wet) (1.0 g) in methanol (40 ml) was hydrogenated under an atmospheric pressure of hydrogen at ambient temperature for 6 hours. The catalyst was filtered off, and the filtrate was evaporated in vacua and dried in vacuo to give 4-(cyclohexyloxy)piperidine (2.42 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06884868B1 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-e3b2890dae964cc2815a21600f6766dd |
| Source note | uspto-grants-2005_04 |