Triethylamine → HCID 22494744, compound

Participants

Reaction Steps

To a solution of 4′-propoxybicyclohexyl-4-ol (1 g) and triethylamine (0.81 ml) in dichloromethane (10 ml) was added dropwise methanesulfonyl chloride (0.39 ml) at 0-5° C., and stirred for 3 hours. The reaction mixture was washed with water and brine, and dried, and evaporated under reduced pressure to give 4′-propoxy-4-methylsulfonyloxy-1,1′-bicyclohexane (1.44 g).

Provenance & Evidence