HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetyl chloride → HCID 68864194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetyl chloride | HCID 89602 | — |
| Reactant | HCID 68866291 | HCID 68866291 | — |
| Product | HCID 68864194 | HCID 68864194 | — |
Reaction Steps
Prepared from (2-amino-5-bromophenyl)(dithien-2-yl)methanol and bromoacetyl chloride using the procedure described in example 1. 1H-NMR (DMSO-d6) δ 10.22 (s, 1H), 8.42 (s, 1H), 8.05 (d, J=9.0 Hz, 1H) 7.59 (m, 3H), 7.05 (m, 2H), 6.87 (m, 2H), 6.78 (d, J=3 Hz, 1H), 3.92 (s, 2H); MS (ES) m/z 484 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598237B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-0754dff38c2f445d8aadbcb31972e151 |
| Source note | uspto-grants-2009_10 |