HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 86598618, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 86598619 | HCID 86598619 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86598618 | HCID 86598618 | 87.4% |
Reaction Steps
A solution of (E)-2,4,6-trimethoxystyryl-3-(acetoxyacetamido)-4-methoxy benzylsulfone (10 mmol) was hydrolyzed in 50% ethanol containing potassium carbonate (70 mmol) to give (E)-2,4,6-trimethoxystyryl-3-(hydroxyacetamido)-4-methoxybenzylsulfone in 87.4% yield. (m.p. 174-1 76° C.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598232B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-73096bf726054bea9e63982e5cdd0001 |
| Source note | uspto-grants-2009_10 |