HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Acetoxypropionyl Chloride → HCID 86598621, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Acetoxypropionyl Chloride | HCID 4547492 | — |
| Reactant | HCID 67401517 | HCID 67401517 | — |
| Product | HCID 86598621 | HCID 86598621 | 68.2% |
Reaction Steps
A solution of 2-acetoxypropionyl chloride (10 mmol) and (E)-2,4,6-trimethoxystyryl-3-amino-4-methoxybenzylsulfone (10 mmol) was reacted according to General Method A. The product obtained was purified by column chromatography to give the desired product in 68.2% yield. (m.p. 179-180° C.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598232B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-d85c05393da54c628a2504d48ae22f5b |
| Source note | uspto-grants-2009_10 |