HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3,6-dioxaheptane → HCID 11691586, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3,6-dioxaheptane | HCID 123532 | — |
| Reactant | HCID 11716432 | HCID 11716432 | — |
| Product | HCID 11691586 | HCID 11691586 | 54.6% |
Reaction Steps
Following the general procedure outlined in Example 7, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)acetonitrile (0.0495 g, 0.164 mmol) and 1-bromo-2-{[2-(methyloxy)ethyl]oxy}ethane (0.040 mL, 0.265 mmol) in 2CH3CN/3CHCl3 (4.0 mL) were reacted to give the desired product (0.0431 g, 54.6%). EI-MS m/z 405 (M+) Rt (1.85 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598267B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-ec1b4a6113774d8aac102fdc6dae81d8 |
| Source note | uspto-grants-2009_10 |