Methylamine → HCID 178485286, compound

HRID 1817267Notes

Reaction equation

HRID 1817267 reaction equation
[N:1]1[C:5]2[CH:6]=[CH:7][C:8]([C:10]([OH:12])=O)=[CH:9][C:4]=2[NH:3][CH:2]=1.[CH3:13][NH2:14]>>[CH3:13][NH:14][C:10]([C:8]1[CH:7]=[CH:6][C:5]2[NH:1][CH:2]=[N:3][C:4]=2[CH:9]=1)=[O:12]

Participants

3

Reactant 2

HCID 6329MethylamineHCID 4594565-Benzimidazolecarboxylic acid

Product 1

HCID 178485286HCID 178485286, compoundYield 67%

Procedure

In a procedure analogous to example 20, reaction of benzimidazole-5-carboxylic acid and aqueous methylamine furnished the product in 67% yield.

Workup

  1. customfurnished the product in 67% yield

Sources & evidence

ORD record
ord-3d932b0917204d34bd43b15c4131ff16
Source dataset
uspto-grants-2009_10
Patent number
US07598272B2

Reaction notes

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