HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10238002, compound → HCID 178467706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10238002 | HCID 10238002 | — |
| Reactant | HCID 178418600 | HCID 178418600 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178467706 | HCID 178467706 | — |
Reaction Steps
2-Ethoxy-3-[4-{3-(4-methanesulfonyloxyphenyl)propylamino}phenyl]propionic acid (100 mg, 1 eq, 0.237 mmol) obtained in Example 15 and L-arginine (41.2 mg, 1 eq, 0.237 mmol) were taken in dry methanol (3 ml), and stirred at RT for 2-3 h. The solvent was removed on rotavapour followed by benzene azeotrope. The residue was dried under high vacuum pump to yield the title compound as a free flowing solid (yield 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598293B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-a771cad2341e47a3b0d009f7c93cab68 |
| Source note | uspto-grants-2009_10 |