HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopropane → 7,7-Dimethyl-5-oxo-2-propylsulfanyl-5,6,7,8-tetrahydroquinoline-3-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopropane | HCID 7840 | — |
| Reactant | 7,7-Dimethyl-5-oxo-2-thioxo-1,2,5,6,7,8-hexahydroquinoline-3-carbonitrile | HCID 1934680 | — |
| Product | 7,7-Dimethyl-5-oxo-2-propylsulfanyl-5,6,7,8-tetrahydroquinoline-3-carbonitrile | HCID 57883307 | 91% |
Reaction Steps
In analogy to the procedure described in Example 1, 7,7-dimethyl-5-oxo-2-thioxo-1,2,5,6,7,8-hexahydroquinoline-3-carbonitrile was treated with 1-bromopropane to give the title compound in 91% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598384B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-576a37b7e11243babcb0bb4d229931e0 |
| Source note | uspto-grants-2009_10 |