HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-7,7-dimethyl-7,8-dihydroquinolin-5(6H)-one → 2-Isobutoxy-7,7-dimethyl-7,8-dihydro-6H-quinolin-5-one hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-7,7-dimethyl-7,8-dihydroquinolin-5(6H)-one | HCID 14812545 | — |
| Solvent | Isobutanol | HCID 6560 | — |
| Product | 2-Isobutoxy-7,7-dimethyl-7,8-dihydro-6H-quinolin-5-one hydrochloride | HCID 69038588 | 35% |
Reaction Steps
In analogy to the procedure described in Example 9, 2-chloro-7,7-dimethyl-7,8-dihydro-6H-quinolin-5-one was treated with iso-butyl alcohol to give the title compound in 35% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598384B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-31f381eb02a646eaaefb6d89be1b36f9 |
| Source note | uspto-grants-2009_10 |