HCID 68869454, compound → 2-Amino-1-(N-cyclopropylmethylamino)-4-(isopropylsulfonyl)benzene

Participants

Reaction Steps

A mixture of N-(cyclopropylmethyl)-4-(isopropylsulfonyl)-2-nitroaniline (Step D, 521 mg, 1.8 mmol) and 10% palladium carbon (52 mg) in methanol (10 mL) and ethyl acetate (10 mL) was stirred at room temperature for 2 h under hydrogen. The mixture was filtered through a pad of celite and the filtrate was concentrated to afford the title compound (462 mg, 98%) as red brown amorphous.

Provenance & Evidence