N,N-Dimethylethylenediamine → N'-[5-(Isopropylsulfonyl)-3-nitropyridin-2-yl]-N,N-dimethylethane-1,2-diamine

HRID 1817875Notes

Reaction equation

HRID 1817875 reaction equation
Cl[C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][C:5]([S:11]([CH:14]([CH3:16])[CH3:15])(=[O:13])=[O:12])=[CH:4][N:3]=1.[CH3:17][N:18]([CH3:22])[CH2:19][CH2:20][NH2:21]>>[CH:14]([S:11]([C:5]1[CH:6]=[C:7]([N+:8]([O-:10])=[O:9])[C:2]([NH:21][CH2:20][CH2:19][N:18]([CH3:22])[CH3:17])=[N:3][CH:4]=1)(=[O:13])=[O:12])([CH3:16])[CH3:15]

Participants

3

Reactant 2

HCID 66053N,N-DimethylethylenediamineHCID 862419792-Chloro-5-(isopropylsulfonyl)-3-nitropyridine

Product 1

HCID 68871359N'-[5-(Isopropylsulfonyl)-3-nitropyridin-2-yl]-N,N-dimethylethane-1,2-diamine

Procedure

The title compound was prepared according to the procedure described in Step A of Example 5 from 2-chloro-5-(isopropylsulfonyl)-3-nitropyridine (Step D of Example 22) and N,N-dimethylethylenediamine.

Sources & evidence

ORD record
ord-31a6fcb040f941e4b81654b4d30f60d5
Source dataset
uspto-grants-2009_10
Patent number
US07598393B2

Reaction notes

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