1-Chloro-4-(ethylsulfonyl)-2-nitrobenzene → HCID 68870024, compound

HRID 1817884Notes

Reaction equation

HRID 1817884 reaction equation
Cl[C:2]1[CH:7]=[CH:6][C:5]([S:8]([CH2:11][CH3:12])(=[O:10])=[O:9])=[CH:4][C:3]=1[N+:13]([O-:15])=[O:14].Cl.[F:17][C:18]([F:24])([F:23])[O:19][CH2:20][CH2:21][NH2:22]>C(N(CC)CC)C>[CH2:11]([S:8]([C:5]1[CH:6]=[CH:7][C:2]([NH:22][CH2:21][CH2:20][O:19][C:18]([F:24])([F:23])[F:17])=[C:3]([N+:13]([O-:15])=[O:14])[CH:4]=1)(=[O:10])=[O:9])[CH3:12]

Participants

4

Reactant 2

HCID 15158591-Chloro-4-(ethylsulfonyl)-2-nitrobenzeneHCID 448908072-(Trifluoromethoxy)ethan-1-amine hydrochloride

Product 1

HCID 68870024HCID 68870024, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The title compound was prepared according to the procedure described in Step A of Example 5 from 1-chloro-4-(ethylsulfonyl)-2-nitrobenzene (Step C of Example 2), 2-(trifluoromethoxy)ethanamine hydrochloride (J. Org. Chem. 2001, 66, 1061-1063.) and triethylamine.

Sources & evidence

ORD record
ord-bb7dc64465da469cbf7a7a812457eddb
Source dataset
uspto-grants-2009_10
Patent number
US07598393B2

Reaction notes

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