HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → 4-Bromo-2-nitro-N-[2-(trifluoromethoxy)ethyl]aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 4-Bromo-1-fluoro-2-nitrobenzene | HCID 2736328 | — |
| Reactant | 2-(Trifluoromethoxy)ethan-1-amine hydrochloride | HCID 44890807 | — |
| Product | 4-Bromo-2-nitro-N-[2-(trifluoromethoxy)ethyl]aniline | HCID 68873547 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Step A of Example 5 from 2-(trifluoromethoxy)ethanamine hydrochloride (J. Org. Chem. 2001, 66, 1061-1063), 4-bromo-1-fluoro-2-nitrobenzene (Wako Pure Chemical Industries, Ltd.) and N,N-diisopropylethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598393B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-31d950ee22ec4e3dafaf373ea9ded853 |
| Source note | uspto-grants-2009_10 |