HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68879380, compound → 1071727-61-1
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68879380 | HCID 68879380 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 1071727-61-1 | HCID 68878048 | — |
Reaction Steps
4-Fluoro-indan-2-carboxylic acid methyl ester in HOAc containing 20% HCl was hydrolyzed according to the protocols as outlined in general procedure G to afford the desired title acid. Spectroscopic data: 1H NMR (300 MHz, DMSO-d6) δ 3.09-3.23 (m, 4H), 3.29-3.40 (m, 1H), 7.0 (t, 1H, J=8.5 Hz), 7.1 (d, 1H, J=7.3 Hz), 7.14-7.24 (m, 1H), 12.4 (br s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598417B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-d8beccfec4dc4e2e9e1336e8887e5666 |
| Source note | uspto-grants-2009_10 |