Triphenylphosphine → HCID 55285106, compound

Participants

Reaction Steps

The title amine was generated from 3-azido-1-ethyl-cyclohexene (2.27 g, 15.00 mmol), triphenyl phosphine (4.00 g, 15.20 mmol) and KOH (0.85 g, 15.20 mmol) according to the protocols as outlined in general procedure I. Spectroscopic data: 1H NMR (300 MHz, CDCl3) δ 0.99 (t, J=7.62 Hz, 3H), 1.09-1.34 (m, 2H), 1.48-1.62 (m, 1H), 1.69-1.79 (m, 1H), 1.83-1.98 (m, 6H), 3.26-3.40 (m, 1H), 5.29-5.38 (m, 1H).

Provenance & Evidence