HRID1818035

反应详情

EQUATION

反应方程式

HRID 1818035 的结构方程式

PROCEDURE

实验过程

The compound was prepared as described in Example 3 by adding cinnamaldehyde (0.048 ml, 0.38 mmol) to N-(cyanoacetyl)benzylamide (Example 4, 0.066 g, 0.38 mmol). After refluxing for 1 h and recrystallization from ethanol a white solid was obtained (0.074 g, 68%). The product gave the following analytical data:

WORKUP

后处理

  1. customThe compound was prepared
  2. temperatureAfter refluxing for 1 h
  3. customrecrystallization from ethanol a white solid
  4. customwas obtained (0.074 g, 68%)
  5. customThe product gave the following analytical data