HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1',1''-(Chlorosilylidyne)tris(benzene) → HCID 11634535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1',1''-(Chlorosilylidyne)tris(benzene) | HCID 6458 | — |
| Reactant | 2',3'-Dideoxy-3'-fluorouridine | HCID 162450 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 11634535 | HCID 11634535 | 60.3% |
Reaction Steps
The title compound was synthesised following a similar procedure as described for Example 11. 3′-Fluoro-2′,3′-dideoxyuridine (0.214 g, 0.93 mmol) was reacted with triphenylsilyl chloride (0.332 g, 1.12 mmol) in dry pyridine (7 mL) for 3 h. to yield the title compound as a white solid (0.274 g, 60%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601702B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-a864f108aaad429ca94cdd3aceef9eda |
| Source note | uspto-grants-2009_10 |