HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trityl chloride → 5-Trityloxypentanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trityl chloride | HCID 6456 | — |
| Reactant | 1,5-Pentanediol | HCID 8105 | — |
| Product | 5-Trityloxypentanol | HCID 11961600 | 24% |
Reaction Steps
The procedure described in example 41 was followed but using 1,5-pentandiol (376 mg, 3.6 mmol) as alcohol instead of cis-2-buten-1,4-diol in the reaction with trityl chloride, which gave the title compound (300 mg, 24%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601702B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-e54e38500dd54cad8827ebf8552e171c |
| Source note | uspto-grants-2009_10 |