HRID1818761

反应详情

EQUATION

反应方程式

HRID 1818761 的结构方程式

PROCEDURE

实验过程

This compound was obtained in 92% yield according to the procedure described in the synthesis of 1-methoxymethylcyclopropylsulfonylamine tert-butylcarbamate (Step B.1.a) except 1.10 equivalents of cyclopropylmethyl bromide were used as electrophile. The compound was taken directly into the next reaction without purification: 1H NMR (CDCl3) δ 0.10 (m, 2H), 0.51 (m, 2H), 0.67 (m, 1H), 1.10 (m, 2H), 1.49 (s, 9H), 1.62 (m, 2H), 1.87 (d, J=7.0 Hz, 2H).

WORKUP

后处理

  1. customThis compound was obtained in 92% yield
  2. customThe compound was taken directly into the next reaction without purification