HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68709452, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 68713725 | HCID 68713725 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 68709452 | HCID 68709452 | — |
Reaction Steps
The clear oil, 1-(tert-butylamino)-4-(2,2-dioxido-3-phenyl-2,1,3-benzothiadiazol-1(3H)-yl)butan-2-one-carbamic acid tert-butyl ester, was dissolved in diethyl ether and methanol and 4N HCl in dioxane was added a precipitate formed. The reaction was filtered to afford 12 mg of 1-(tert-butylamino)-4-(2,2-dioxido-3-phenyl-2,1,3-benzothiadiazol-1(3H)-yl)butan-2-one hydrochloride as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601722B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-7b3a132ce0eb4c5d9108d0f003149a40 |
| Source note | uspto-grants-2009_10 |