HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68422863, compound → HCID 68425439, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68422863 | HCID 68422863 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol--water (1/1) | HCID 22242641 | — |
| Product | HCID 68425439 | HCID 68425439 | — |
Reaction Steps
Compound 7.3 (1.0 mmol) and Pd/C (10 w/w %, 60 mg) in MeOH—H2O (12 mL) is stirred under a hydrogen atmosphere at room temperature until the reaction is complete. The catalyst is removed by filtration and the filtrate is evaporated to dryness under reduced pressure to provide thieno[3,2-d]pyrimidine-4-carboxylic acid 4-amino-benzylamide (compound 7.4).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601725B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-4dd7e502aae74e529d34d5d8e4d3798e |
| Source note | uspto-grants-2009_10 |