HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Octene → Tetradec-7-ene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Octene | HCID 8125 | — |
| Catalyst | HCID 178479819 | HCID 178479819 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | Tetradec-7-ene | HCID 25209 | 80% |
Reaction Steps
A mixture of 1-octene (7.15 g, 64 mmol) and Grubbs' catalyst (0.030 g, 0.04 mmol, 0.0006 equ) was stirred under a static vacuum for 15 hours, then passed through a plug of silica eluting with hexane. Concentration gave tetradec-7-ene (4.982 g, 80%) as a colourless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601754B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-059bfbb3bdb943b8b53ba4481f757dce |
| Source note | uspto-grants-2009_10 |