Triethylamine → HCID 24899700, compound

Participants

Reaction Steps

Following the procedure of Example 1, tetrahydro-dibenzofuran-2-ylamine (2.8 g, 15 mmol), 4-nitrobenzoyl chloride (3.0 g, 16 mmol), and triethylamine (6.4 mL, 45 mmol) in tetrahydrofuran (60 mL) provided 4-nitro-N-(6,7,8,9-tetrahydro-dibenzofuran-2-yl)-benzamide (4.1 g). Mp 279-280° C.;Anal. Calcd. for C19H16N2O4: C, 67.85; H, 4.79; N, 8.33; Found: C, 67.69; H, 4.61; N, 8.26.

Provenance & Evidence