HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 24899703, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 21221605 | HCID 21221605 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 24899703 | HCID 24899703 | 51.5% |
Reaction Steps
Following the procedure of Example 1, tetrahydro-dibenzofuran-2-ylamine (0.94 g, 5.0 mmol) and benzoyl chloride (0.64 mL, 5.5 mmol) in pyridine (10 mL) provided N-(6,7,8,9-tetrahydro-dibenzofuran-2-yl)-benzamide (0.75 g). Mp 178-180° C.; Anal. Calcd. for C19H17NO2: C, 78.33; H, 5.88; N, 4.81; Found: C, 78.10; H, 5.86; N, 4.81.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601856B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-ac2a5d07e78f40788d857dae03b97cd0 |
| Source note | uspto-grants-2009_10 |