HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexanoyl chloride → HCID 24899706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexanoyl chloride | HCID 67340 | — |
| Reactant | HCID 21221605 | HCID 21221605 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 24899706 | HCID 24899706 | 43.8% |
Reaction Steps
Following the procedure of Example 23, tetrahydro-dibenzofuran-2-ylamine (0.15 g, 0.80 mmol), hexanoyl chloride (0.11 mL, 0.80 mmol), and poly(vinylpyridine) (0.5 g) in dichloroethane (8 mL) provided N-(6,7,8,9-tetrahydrodibenzo[b,d]furan-2-yl)hexanamide (0.10 g). MS (ESI) m/z286.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601856B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-d0f4cc2ab53d4023bd9fb50a0469f517 |
| Source note | uspto-grants-2009_10 |