Cyclohexylacetyl chloride → HCID 24899956, compound

Participants

Reaction Steps

Following the procedure of Example 1, 7,8,9,10-tetrahydro-6H-benzo[b]-cyclohepta[d]furan-2-ylamine (0.91 g, 4.5 mmol) and cyclohexylacetyl chloride (0.80 g, 5.0 mmol) in pyridine (10 mL) provided 2-cyclohexyl-N-[7,8,9,10-tetrahydro-6H-benzo[b]-cyclohepta[d]furan-2-yl]acetamide (0.53 g). Mp 188-189° C.; Anal. Calcd. for C21H27NO2: C, 77.50; H, 8.36; N, 4.30; Found: C, 77.51; H, 8.43; N, 4.32.

Provenance & Evidence