HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Cyclopentylpropionyl chloride → HCID 24897638, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Cyclopentylpropionyl chloride | HCID 66039 | — |
| Reactant | HCID 57890287 | HCID 57890287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 24897638 | HCID 24897638 | 63.8% |
Reaction Steps
Following the procedure of Example 1, 6,7,8,9,10,11-Hexahydro-benzo[b]-cycloocta[d]furan-2-ylamine (0.13 g, 0.60 mmol), 3-cyclopentylpropionyl chloride (0.10 g, 0.63 mmol), and poly(vinylpyridine) (0.5 g) in dichloromethane (15 mL) provided 3-cyclopentyl-N-(6,7,8,9,10,11-hexahydrobenzo[b]cycloocta[d]furan-2-yl)propanamide (0.13 g). MS (ESI) m/z 340 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601856B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-f17506219e01424f82e130bca0d40237 |
| Source note | uspto-grants-2009_10 |