Hexanoyl chloride → HCID 24897634, compound

Participants

Reaction Steps

Following the procedure of Example 1, 6,7,8,9,10,11-Hexahydro-benzo[b]-cycloocta[d]furan-2-ylamine (0.15 g, 0.69 mmol), hexanoyl chloride (0.098 mL, 0.69 mmol), and poly(vinylpyridine) (0.5 g) in dichloroethane (8 mL) provided N-(6,7,8,9,10,11-hexahydrobenzo[b]cycloocta[d]furan-2-yl)hexanamide (0.10 g). MS (ESI) m/z 314 ([M+H]+).

Provenance & Evidence