HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 24897636, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 57890287 | HCID 57890287 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 24897636 | HCID 24897636 | 56.3% |
Reaction Steps
Following the procedure of Example 1, 6,7,8,9,10,11-Hexahydro-benzo[b]-cycloocta[d]furan-2-ylamine (0.15 g, 0.69 mmol), acetyl chloride (0.055 mL, 0.69 mmol), and poly(vinylpyridine) (0.5 g) in dichloroethane (8 mL) provided N-(6,7,8,9,10,11-hexahydrobenzo[b]cycloocta[d]furan-2-yl)acetamide (0.10 g). MS (ESI) m/z 258 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601856B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-494217b6d5a9472090ed510bc2fa45bc |
| Source note | uspto-grants-2009_10 |