HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetyl chloride → HCID 24897639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetyl chloride | HCID 7679 | — |
| Reactant | HCID 57890287 | HCID 57890287 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 24897639 | HCID 24897639 | 81.5% |
Reaction Steps
Following the procedure of Example 1, 6,7,8,9,10,11-Hexahydro-benzo[b]-cycloocta[d]furan-2-ylamine (0.20 g, 0.92 mmol), phenylacetyl chloride (0.14 mL, 1.0 mmol), and poly(vinylpyridine) (0.5 g) in dichloroethane (12 mL) provided N-(6,7,8,9,10,11-hexahydrobenzo[b]cycloocta[d]furan-2-yl)-2-phenylacetamide (0.25 g). MS (ESI) m/z 334.3 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601856B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-dc7daa821bb9444195114a97293e310f |
| Source note | uspto-grants-2009_10 |