2,6-Dimethoxybenzoyl chloride → HCID 24897851, compound

Participants

Reaction Steps

Following the procedure of Example 1, 6,7,8,9,10,11-Hexahydro-benzo[b]-cycloocta[d]furan-2-ylamine (0.15 g, 0.69 mmol), 2,6-dimethoxybenzoyl chloride (0.15 mL, 0.77 mmol), and poly(vinylpyridine) (0.5 g) in dichloroethane (12 mL) N-(6,7,8,9,10,11-hexahydrobenzo[b]cycloocta[d]furan-2-yl)-2,6-dimethoxybenzamide (0.15 g). MS (ESI) m/z 380 ([M+H]+).

Provenance & Evidence