HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isonicotinoyl chloride hydrochloride → HCID 24897852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isonicotinoyl chloride hydrochloride | HCID 12262826 | — |
| Reactant | HCID 57890287 | HCID 57890287 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 24897852 | HCID 24897852 | 44.1% |
Reaction Steps
Following the procedure of Example 1, 6,7,8,9,10,11-Hexahydro-benzo[b]-cycloocta[d]furan-2-ylamine (0.20 g, 0.92 mmol), isonicotinoyl chloride hydrochloride (0.20 g, 1.1 mmol), and poly(vinylpyridine) (0.5 g) in dichloroethane (12 mL) provided N-(6,7,8,9,10,11-hexahydrobenzo[b]cycloocta[d]furan-2-yl)isonicotinamide (0.13 g). MS (ESI) m/z 321 ([M+H]+); MS (ESI) m/z 319 ([M−H]−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601856B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-ec8eb8b3ebc94879984a1b2a8c48ea7f |
| Source note | uspto-grants-2009_10 |